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Oxidation Behaviour of Al-Si Coating after Diffusion under Different Conditions |
Received:November 01, 2018 Revised:January 25, 2019 |
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DOI:10.7643/ issn.1672-9242.2019.01.006 |
KeyWord:Al-Si coating oxidation SEM EDS |
Author | Institution |
CHEN Zhong |
AECC Guiyang Precision Casting Company, Guiyang , China |
MENG Cai-si |
AECC Guiyang Precision Casting Company, Guiyang , China |
HUO Ke-li |
AECC Guiyang Precision Casting Company, Guiyang , China |
ZHANG Yao |
AECC Guiyang Precision Casting Company, Guiyang , China |
HAO Fen-li |
AECC Guiyang Precision Casting Company, Guiyang , China |
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Abstract: |
Objective To improve the oxidation resistance of Al-Si coating. Methods Al-Si protective coatings were prepared on the gas flowing surface of directional freezing DZ417G Ni-superalloy blade by slurry method. The surface microstructure and cross-sectional microstructure of the coatings were analyzed by scanning electron microscopy (SEM). Results In the diffusion process of Al-Si coating without protective atmosphere, the porous and non-dense phase of θ-Al2O3 was formed firstly. With the oxidation process proceeding, θ-Al2O3 phase gradually transformed into dense structure of α-Al2O3 phase, which had the real oxidation resistance. Conclusion The Al element in the Al-Si coating is consumed in advance, which has certain influence on the service life of the Al-Si coating. Therefore, diffusion process after infiltration must be carried out in vacuum or in protective atmosphere. Then the Al concentration can meet requirement and α-Al2O3 phase can form in the application process for oxidation resistance and thus improve the service life of the blade. |
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